BMRB Entry 26056
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PDB ID:
Entry in NMR Restraints Grid
Validation report in NRG-CING
Chem Shift validation: AVS_full, SPARTA
BMRB Entry DOI: doi:10.13018/BMR26056
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Title: SOLUTION STRUCTURE OF HELATX1
Deposition date: 2016-05-12 Original release date: 2017-05-30
Authors: PARK, BONG GYU; KIM, JAE IL
Citation: PARK, BONG GYU; KIM, JAE IL. "SOLUTION STRUCTURE OF HELATX1" Biochim. Biophys. Acta ., .-..
Assembly members:
entity, polymer, 25 residues, 2932.458 Da.
Natural source: Common Name: scorpions Taxonomy ID: 217256 Superkingdom: Eukaryota Kingdom: Metazoa Genus/species: Heterometrus laoticus
Experimental source: Production method: recombinant technology Host organism: Synthetic peptide
Entity Sequences (FASTA):
entity: SCKKECSGSRRTKKCMQKCN
REHGH
- assigned_chemical_shifts
| Data type | Count |
| 1H chemical shifts | 128 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | entity | 1 |
Entities:
Entity 1, entity 25 residues - 2932.458 Da.
| 1 | SER | CYS | LYS | LYS | GLU | CYS | SER | GLY | SER | ARG | ||||
| 2 | ARG | THR | LYS | LYS | CYS | MET | GLN | LYS | CYS | ASN | ||||
| 3 | ARG | GLU | HIS | GLY | HIS |
Samples:
sample_1: H2O 90%; D2O, [U-100% 2H], 10%
sample_conditions_1: pH: 4.0; pressure: 1 atm; temperature: 288 K
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| 2D 1H-1H TOCSY | sample_1 | isotropic | sample_conditions_1 |
| 2D 1H-1H COSY | sample_1 | isotropic | sample_conditions_1 |
| 2D 1H-1H NOESY | sample_1 | isotropic | sample_conditions_1 |
Software:
CYANA, Guntert, Mumenthaler and Wuthrich - chemical shift assignment
NMR spectrometers:
- Bruker Avance 600 MHz