BMRB Entry 25201
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PDB ID:
Entry in NMR Restraints Grid
Validation report in NRG-CING
Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR25201
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Title: Shortening and modifying the 1513 MSP-1 peptide's alpha-helical region induces protection against malaria
Deposition date: 2014-09-04 Original release date: 2014-11-10
Authors: Espejo, Fabiola; Bermudez, Adriana; Torres, Elizabeth; Urquiza, Mauricio; Rodriguez, Raul; Lopez, Yolanda; Patarroyo, Manuel Elkin
Citation: Espejo, Fabiola; Bermudez, Adriana; Torres, Elizabeth; Urquiza, Mauricio; Rodriguez, Raul; Lopez, Yolanda; Patarroyo, Manuel Elkin. "Shortening modifying the 1513 MSP-1 peptide's alpha-helical region induces protection against malaria" Biochem. Biophys. Res. Commun. ., .-..
Assembly members:
entity, polymer, 20 residues, 2162.436 Da.
Natural source: Common Name: not available Taxonomy ID: not available Superkingdom: not available Kingdom: not available Genus/species: not available not available
Experimental source: Production method: chemical synthesis
Entity Sequences (FASTA):
entity: GYSLFQKEKMVLNEGTSGTA
- assigned_chemical_shifts
| Data type | Count |
| 1H chemical shifts | 127 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | entity | 1 |
Entities:
Entity 1, entity 20 residues - 2162.436 Da.
| 1 | GLY | TYR | SER | LEU | PHE | GLN | LYS | GLU | LYS | MET | |
| 2 | VAL | LEU | ASN | GLU | GLY | THR | SER | GLY | THR | ALA |
Samples:
sample_1: entity 8 mM; H2O 70%; trifluoroethanol 30%
sample_conditions_1: temperature: 295 K; pH: 3.7; pressure: 1 atm
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| 2D DQF-COSY | sample_1 | isotropic | sample_conditions_1 |
| 2D 1H-1H TOCSY | sample_1 | isotropic | sample_conditions_1 |
| 2D 1H-1H NOESY | sample_1 | isotropic | sample_conditions_1 |
Software:
InsightII, Accelrys Software Inc. - geometry optimization, refinement
NMR spectrometers:
- Bruker DRX 600 MHz