BMRB Entry 15390
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PDB ID:
Entry in NMR Restraints Grid
Validation report in NRG-CING
Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR15390
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Title: Influenza Hemagglutinin Fusion Domain Mutant F9A PubMed: 17567572
Deposition date: 2007-07-18 Original release date: 2008-06-18
Authors: Lai, Alex; Tamm, Lukas
Citation: Lai, Alex; Tamm, Lukas. "Locking the kink in the influenza hemagglutinin fusion domain structure." J. Biol. Chem. 282, 23946-23956 (2007).
Assembly members:
HA_FP_F9A, polymer, 27 residues, 1978.201 Da.
Natural source: Common Name: Influenza virus Taxonomy ID: 11309 Superkingdom: Viruses Kingdom: not available Genus/species: not available Influenza Virus A
Experimental source: Production method: chemical synthesis Host organism: N.A.
Entity Sequences (FASTA):
HA_FP_F9A: GLFGAIAGAIENGWEGMIDG
GCGKKKK
- assigned_chemical_shifts
| Data type | Count |
| 1H chemical shifts | 122 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | HA FP F9A | 1 |
Entities:
Entity 1, HA FP F9A 27 residues - 1978.201 Da.
| 1 | GLY | LEU | PHE | GLY | ALA | ILE | ALA | GLY | ALA | ILE | ||||
| 2 | GLU | ASN | GLY | TRP | GLU | GLY | MET | ILE | ASP | GLY | ||||
| 3 | GLY | CYS | GLY | LYS | LYS | LYS | LYS |
Samples:
sample_1: HA_FP_F9A peptide 2 mM; d38-DPC, [U-2H], 200 mM; MES 5 mM; HEPES 10 mM; DTT 5 mM; NaN3 0.05 % (w:v)
sample_conditions_1: pH: 5; pressure: 1 atm; temperature: 303 K
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| 2D 1H-1H NOESY | sample_1 | isotropic | sample_conditions_1 |
| 2D 1H-1H TOCSY | sample_1 | isotropic | sample_conditions_1 |
Software:
NMRPipe, Delaglio, Grzesiek, Vuister, Zhu, Pfeifer and Bax - processing
DYANA, Guntert, Braun and Wuthrich - structure solution
OPAL, Luginbuhl, Guntert, Billeter and Wuthrich - refinement
SPARKY, Goddard - chemical shift assignment
NMR spectrometers:
- Varian INOVA 600 MHz
Related Database Links:
| PDB |